10.48349/ASU/SCXUIW Jamboretz, John John Jamboretz https://orcid.org/0000-0001-6736-4130 Arizona State University Birkel, Christina Christina Birkel https://orcid.org/0000-0001-8979-5214 Arizona State University ASU Library Research Data Repository 2022 Chemistry Raman spectroscopy Microwave heating Inorganic compounds--Synthesis School of Molecular Sciences Arizona State University Jamboretz, John John Jamboretz Arizona State University Birkel, Christina Christina Birkel Arizona State University 2022-06-17 2022-09-20 2022-10-14 2022-02-11/2022-02-14 286445 38708224 93372784 27977461 69731128 12195 3070 182809 3727 3622 3691 3685 7566 213125 7705 text/tab-separated-values text/csv text/csv text/csv text/csv text/tab-separated-values application/octet-stream application/octet-stream application/octet-stream application/octet-stream application/octet-stream application/octet-stream text/plain application/octet-stream text/plain 2.0 CC0 1.0 <p>TiO2 anatase to rutile proof-of-concept study</p> <p>In situ Raman spectroscopic data for the observation of a phase change in TiO2 (titania) from anatase to rutile. These data sets are the results of a proof-of-concept study for a custom Raman instrument which was built for the purpose of observing inorganic transformation under microwave heating and at high temperatures in the standard synthetic laboratory environment. They demonstrate the ability of the new instrument to observe these transformations in real-time and gain a better understanding of microwave heating methods for inorganic synthesis. It is relevant to Raman spectroscopists and inorganic synthetic chemists, especially those specializing in microwave processing.</p> <p>Dataset contains 7 delimited data files (.csv, .tab) and 6 MATLAB live scripts (.mlx).</p> <p>See <a href="https://dataverse.asu.edu/file.xhtml?fileId=27565">README</a> for additional information.</p> Matlab, R2021B (Mathworks) Excel, null GRBL, https://github.com/grbl/grbl Tempe, Arizona, United States