Replication Data for: In situ Raman Spectroscopy of Microwave Synthesis of Inorganic Compoundsdoi:10.48349/ASU/SCXUIWASU Library Research Data Repository2022-09-202Jamboretz, John; Birkel, Christina, 2022, "Replication Data for: In situ Raman Spectroscopy of Microwave Synthesis of Inorganic Compounds", https://doi.org/10.48349/ASU/SCXUIW, ASU Library Research Data Repository, V2, UNF:6:ZIgINeG56JeEGPZucA8zmw== [fileUNF]Replication Data for: In situ Raman Spectroscopy of Microwave Synthesis of Inorganic CompoundsTiO2 anatase to rutile proof-of-concept studydoi:10.48349/ASU/SCXUIWJamboretz, JohnBirkel, ChristinaSchool of Molecular SciencesTempe, Arizona, United StatesMatlabExcelGRBLASU Library Research Data RepositoryJamboretz, JohnBirkel, ChristinaJamboretz, John2022-06-17ChemistryRaman spectroscopyMicrowave heatingInorganic compounds--Synthesis<p>TiO2 anatase to rutile proof-of-concept study</p> <p>In situ Raman spectroscopic data for the observation of a phase change in TiO2 (titania) from anatase to rutile. These data sets are the results of a proof-of-concept study for a custom Raman instrument which was built for the purpose of observing inorganic transformation under microwave heating and at high temperatures in the standard synthetic laboratory environment. They demonstrate the ability of the new instrument to observe these transformations in real-time and gain a better understanding of microwave heating methods for inorganic synthesis. It is relevant to Raman spectroscopists and inorganic synthetic chemists, especially those specializing in microwave processing.</p> <p>Dataset contains 7 delimited data files (.csv, .tab) and 6 MATLAB live scripts (.mlx).</p> <p>See <a href="https://dataverse.asu.edu/file.xhtml?fileId=27565">README</a> for additional information.</p>2022-02-112022-02-14Jamboretz, J., Reitz, A., and Birkel, C. (under review) Development of a Raman spectroscopy system for in situ monitoring of microwave-assisted inorganic transformations. - Manuscript under reviewJamboretz, J., Reitz, A., and Birkel, C. (under review) Development of a Raman spectroscopy system for in situ monitoring of microwave-assisted inorganic transformations. - Manuscript under review600nmcenter_relativewavenumbermap.tab10231text/tab-separated-valuesUNF:6:2r4GUIobEmzLbovxzLS4EA==JJ196_rawtemperaturedata.tab129992text/tab-separated-valuesUNF:6:gHDmup4WJATINuFGhcJRug==-37.514422341117.12283545941481023.02057.440701048478.2134.076223-32.734490563840.6260960.0UNF:6:2r4GUIobEmzLbovxzLS4EA==12.0.13000.012999.03752.6324093894410.06501.06501.0UNF:6:n1cC8UFxK8Lvti4+AGJD5w==97.9253071661901859.103612306203294.634760988120612999.0443.135302382286491.597090949112597.9387861974570.0.UNF:6:PJ+qFwQpa0TzE55dab3iWg==importandprocessfunc.mlxapplication/octet-streamJamboretzJohn_InsituRamanSpectroscopyMicrowave_SynthesisInorganicCompounds_README_v1.txttext/plainJJ192_rawbackgrounddata.csvtext/csvJJ192_rawspectraldata.csvtext/csvJJ196_rawbackgrounddata.csvtext/csvJJ196_rawspectraldata.csvtext/csvrasterfunc.mlxapplication/octet-streamstartexperiment.mlxapplication/octet-streamstartexperimentfunc.mlxapplication/octet-streamthermocouplefunc.mlxapplication/octet-streamtransitionchangepointexample.mlxapplication/octet-stream