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Part 1: Document Description
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Citation |
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Title: |
Replication Data for: In situ Raman Spectroscopy of Microwave Synthesis of Inorganic Compounds |
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Identification Number: |
doi:10.48349/ASU/SCXUIW |
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Distributor: |
ASU Library Research Data Repository |
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Date of Distribution: |
2022-09-20 |
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Version: |
2 |
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Bibliographic Citation: |
Jamboretz, John; Birkel, Christina, 2022, "Replication Data for: In situ Raman Spectroscopy of Microwave Synthesis of Inorganic Compounds", https://doi.org/10.48349/ASU/SCXUIW, ASU Library Research Data Repository, V2, UNF:6:ZIgINeG56JeEGPZucA8zmw== [fileUNF] |
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Citation |
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Title: |
Replication Data for: In situ Raman Spectroscopy of Microwave Synthesis of Inorganic Compounds |
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Subtitle: |
TiO2 anatase to rutile proof-of-concept study |
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Identification Number: |
doi:10.48349/ASU/SCXUIW |
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Authoring Entity: |
Jamboretz, John (Arizona State University) |
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Birkel, Christina (Arizona State University) |
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Producer: |
School of Molecular Sciences |
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Software used in Production: |
Matlab |
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Software used in Production: |
Excel |
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Software used in Production: |
GRBL |
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Distributor: |
ASU Library Research Data Repository |
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Access Authority: |
Jamboretz, John |
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Access Authority: |
Birkel, Christina |
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Depositor: |
Jamboretz, John |
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Date of Deposit: |
2022-06-17 |
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Holdings Information: |
https://doi.org/10.48349/ASU/SCXUIW |
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Study Scope |
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Keywords: |
Chemistry, Raman spectroscopy, Microwave heating, Inorganic compounds--Synthesis |
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Abstract: |
<p>TiO2 anatase to rutile proof-of-concept study</p> <p>In situ Raman spectroscopic data for the observation of a phase change in TiO2 (titania) from anatase to rutile. These data sets are the results of a proof-of-concept study for a custom Raman instrument which was built for the purpose of observing inorganic transformation under microwave heating and at high temperatures in the standard synthetic laboratory environment. They demonstrate the ability of the new instrument to observe these transformations in real-time and gain a better understanding of microwave heating methods for inorganic synthesis. It is relevant to Raman spectroscopists and inorganic synthetic chemists, especially those specializing in microwave processing.</p> <p>Dataset contains 7 delimited data files (.csv, .tab) and 6 MATLAB live scripts (.mlx).</p> <p>See <a href="https://dataverse.asu.edu/file.xhtml?fileId=27565">README</a> for additional information.</p> |
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Date of Collection: |
2022-02-11-2022-02-14 |
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Methodology and Processing |
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Sources Statement |
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Data Access |
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Other Study Description Materials |
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Related Publications |
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Citation |
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Title: |
Jamboretz, J., Reitz, A., and Birkel, C. (under review) Development of a Raman spectroscopy system for in situ monitoring of microwave-assisted inorganic transformations. - Manuscript under review |
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Bibliographic Citation: |
Jamboretz, J., Reitz, A., and Birkel, C. (under review) Development of a Raman spectroscopy system for in situ monitoring of microwave-assisted inorganic transformations. - Manuscript under review |
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File Description--f10148 |
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File: 600nmcenter_relativewavenumbermap.tab |
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Notes: |
UNF:6:2r4GUIobEmzLbovxzLS4EA== |
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File Description--f10142 |
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File: JJ196_rawtemperaturedata.tab |
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Notes: |
UNF:6:gHDmup4WJATINuFGhcJRug== |
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List of Variables: |
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Variables |
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f10148 Location: |
Summary Statistics: StDev 1117.1228354594148; Valid 1023.0; Mean 2057.440701048478; Min. -32.73449056; Max. 3840.626096; Variable Format: numeric Notes: UNF:6:2r4GUIobEmzLbovxzLS4EA== |
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f10142 Location: |
Summary Statistics: Min. 2.0; Max. 13000.0; Valid 12999.0; StDev 3752.632409389441; Mean 6501.0; Variable Format: numeric Notes: UNF:6:n1cC8UFxK8Lvti4+AGJD5w== |
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f10142 Location: |
Summary Statistics: Max. 859.103612306203; StDev 294.6347609881206; Valid 12999.0; Mean 491.5970909491125; Min. 97.938786197457; Variable Format: numeric Notes: UNF:6:PJ+qFwQpa0TzE55dab3iWg== |
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Label: |
importandprocessfunc.mlx |
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Notes: |
application/octet-stream |
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Label: |
JamboretzJohn_InsituRamanSpectroscopyMicrowave_SynthesisInorganicCompounds_README_v1.txt |
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Notes: |
text/plain |
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Label: |
JJ192_rawbackgrounddata.csv |
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Notes: |
text/csv |
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Label: |
JJ192_rawspectraldata.csv |
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Notes: |
text/csv |
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Label: |
JJ196_rawbackgrounddata.csv |
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Notes: |
text/csv |
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Label: |
JJ196_rawspectraldata.csv |
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Notes: |
text/csv |
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Label: |
rasterfunc.mlx |
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Notes: |
application/octet-stream |
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Label: |
startexperiment.mlx |
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Notes: |
application/octet-stream |
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Label: |
startexperimentfunc.mlx |
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Notes: |
application/octet-stream |
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Label: |
thermocouplefunc.mlx |
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Notes: |
application/octet-stream |
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Label: |
transitionchangepointexample.mlx |
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Notes: |
application/octet-stream |